Thortveitite-type Tm2Si2O7
Identifieur interne : 000241 ( Main/Exploration ); précédent : 000240; suivant : 000242Thortveitite-type Tm2Si2O7
Auteurs : Volker Kahlenberg [Autriche] ; Paul Aichholzer [Autriche]Source :
- Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2014.
Abstract
Single crystals of dithulium disilicate, Tm2Si2O7, were obtained in flux synthesis experiments in the system SiO2–Tm2O3–LiF at ambient pressure. The compound belongs to the group of sorosilicates,
Url:
DOI: 10.1107/S1600536814013142
PubMed: 25161507
PubMed Central: 4120532
Affiliations:
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Le document en format XML
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Si<sub>2</sub>
O<sub>7</sub>
</title>
<author><name sortKey="Kahlenberg, Volker" sort="Kahlenberg, Volker" uniqKey="Kahlenberg V" first="Volker" last="Kahlenberg">Volker Kahlenberg</name>
<affiliation wicri:level="1"><nlm:aff id="a">University of Innsbruck, Institute of Mineralogy & Petrography, Innrain 52, A-6020 Innsbruck,<country>Austria</country>
</nlm:aff>
<country xml:lang="fr">Autriche</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<author><name sortKey="Aichholzer, Paul" sort="Aichholzer, Paul" uniqKey="Aichholzer P" first="Paul" last="Aichholzer">Paul Aichholzer</name>
<affiliation wicri:level="1"><nlm:aff id="a">University of Innsbruck, Institute of Mineralogy & Petrography, Innrain 52, A-6020 Innsbruck,<country>Austria</country>
</nlm:aff>
<country xml:lang="fr">Autriche</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Thortveitite-type Tm<sub>2</sub>
Si<sub>2</sub>
O<sub>7</sub>
</title>
<author><name sortKey="Kahlenberg, Volker" sort="Kahlenberg, Volker" uniqKey="Kahlenberg V" first="Volker" last="Kahlenberg">Volker Kahlenberg</name>
<affiliation wicri:level="1"><nlm:aff id="a">University of Innsbruck, Institute of Mineralogy & Petrography, Innrain 52, A-6020 Innsbruck,<country>Austria</country>
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<country xml:lang="fr">Autriche</country>
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<author><name sortKey="Aichholzer, Paul" sort="Aichholzer, Paul" uniqKey="Aichholzer P" first="Paul" last="Aichholzer">Paul Aichholzer</name>
<affiliation wicri:level="1"><nlm:aff id="a">University of Innsbruck, Institute of Mineralogy & Petrography, Innrain 52, A-6020 Innsbruck,<country>Austria</country>
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<country xml:lang="fr">Autriche</country>
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<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
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<front><div type="abstract" xml:lang="en"><p>Single crystals of dithulium disilicate, Tm<sub>2</sub>
Si<sub>2</sub>
O<sub>7</sub>
, were obtained in flux synthesis experiments in the system SiO<sub>2</sub>
–Tm<sub>2</sub>
O<sub>3</sub>
–LiF at ambient pressure. The compound belongs to the group of sorosilicates, <italic>i.e.</italic>
it is based on [Si<sub>2</sub>
O<sub>7</sub>
]-units and crystallizes in the thortveitite (Sc<sub>2</sub>
Si<sub>2</sub>
O<sub>7</sub>
) structure type. The Tm<sup>3+</sup>
cation (site symmetry .2.) occupies a distorted octahedral site, with Tm—O bond lengths in the range 2.217 (4)–2.289 (4) Å. Each of the octahedra shares three of its edges with adjacent [TmO<sub>6</sub>
] groups, resulting in the formation of layers parallel to (001). The individual [SiO<sub>4</sub>
] tetrahedra are more regular, <italic>i.e.</italic>
the differences between the bond lengths between Si and the bridging and non-bridging O atoms are not very pronounced. The layers containing the octahedra and the sheets containing the [Si<sub>2</sub>
O<sub>7</sub>
] groups (point group symmetry 2/<italic>m</italic>
) form an alternating sequence. Linkage is provided by sharing common oxygen vertices.</p>
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